Synthesis of an anion receptor using 3,6-diaminophenanthrene as a scaffold

<p>1H and 13C NMR spectra for the compounds:</p> <ul> <li>2-iodo-4-nitrobenzoic acid (<strong>6</strong>)</li> <li>(2-iodo-4-nitrophenyl)methanol (<strong>7</strong>)</li> <li>2-iodo-4-nitrobenzaldehyde (<strong>8</strong>)</li> <li>5,5'-dinitro-[1,1'-biphenyl]-2,2'-dicarbaldehyde (<strong>9</strong>)</li> <li>3,6-dinitrophenanthrene (<strong>10</strong>)</li> <li>3,6-diaminophenanthrene (<strong>11</strong>)</li> <li>1,1'-(phenanthrene-3,6-diyl)bis(3-(3,5-bis(trifluoromethyl)phenyl)urea) (<strong>13</strong>)</li> </ul> <p>MNOVA files for the compounds are provided, as well as the original files recorded on a 400MHz JEOL NMR spectrometer in jdf format.</p>