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Data from: Enhancement of apoptosis by titanium alloy internal fixations during microwave treatments for fractures: an animal study
Objective: Microwaves are used in one method of physical therapy and can increase muscle tissue temperature which is useful for improving muscle, tendon and bone injuries. In the study, we sought to determine whether titanium alloy internal fixations influence apoptosis in tissues subjected to microwave treatments at 2,450 MHz and 40 W during the healing of fractures because this issue is not yet fully understood. Methods: In this study, titanium alloy internal fixations were used to treat 3.0-mm transverse osteotomies in the middle of New Zealand rabbits' femurs. After the operation, 30-day microwave treatments were applied to the 3.0 mm transverse osteotomies 3 days after the operation. The changes in the temperatures of the muscle tissues in front of the implants or the 3.0 mm transverse osteotomies were measured during the microwave treatments. To characterize the effects of titanium alloy internal fixations on apoptosis in the muscles after microwave treatment, we performed TUNEL assays, fluorescent real-time (quantitative) PCR, western blotting analyses, reactive oxygen species (ROS) detection and transmission electron microscopy examinations. Results: The temperatures were markedly increased in the animals with the titanium alloy implants. Apoptosis in the muscle cells of the implanted group was significantly more extensive than that in the non-implanted control group at different time points. Transmission electron microscopy examinations of the skeletal muscles of the implanted groups revealed muscular mitochondrial swelling, vacuolization. ROS, Bax and Hsp70 were up-regulated, and Bcl-2 was down-regulated in the implanted group. Conclusion: Our results suggest that titanium alloy internal fixations caused greater muscular tissue cell apoptosis following 2,450 MHz, 40 W microwave treatments in this rabbit femur fracture models.
Scheme 4 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 4 Microwave irradiated condensation of diketone with primary amine.
Scheme 1 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 1 General Paal-Knorr synthesis of pyrroles.
Figure 4 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Figure 4 Chemical reactions of the pyrrole.
Scheme 22 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 22 Synthesis of N-substituted pyrrole derivatives with nanocatalysts or MW.
Scheme 11 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 11 Microwave-Assisted Sila-Stetter/Paal-Knorr Reaction
Scheme 18 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 18 Clauson-Kaas synthesis of pyrroles catalyzed by [hmim][HSO4].
Figure 1 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Figure 1 Electromagnetic spectrum.
Scheme 10 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 10 Nano-organocatalyst promoted Paal-Knorr reaction.
Scheme 14 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 14 Paal-Knorr MW synthesis in the presence of alkaline salts as catalysts.
Scheme 25 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 25 MW assisted synthesis of 1,2-disubstituted pyrroles on the surface of silica gel.
Scheme 17 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 17 Synthesis of 2-pyrrolin-5-ones by Hantzsch-type reaction.
Scheme 24 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 24 MW irradiated synthesis of functionalized pyrroles using UO2(NO3).6H2O as a catalyst.
Scheme 7 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 7 MW synthesis of pyrroles from diketons and acetic acid.
Figure 2 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Figure 2 Major advantages of MW assisted synthesis.
Scheme 16 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 16 Solvent-free MW synthesis of pyrroles with organocatalyst.
Scheme 21 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 21 Solvent-free synthesis of novel sulfonylpyrroles by MW heating.
Scheme 13 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 13 Synthesis of Tetra-substituted Pyrrole Amide Library.
Scheme 19 from: Mateev E, Irfan A, Mateeva A, Georgieva M, Zlatkov A (2024) Microwave-assisted organic synthesis of pyrroles (Review). Pharmacia 71: 1-10. https://doi.org/10.3897/pharmacia.71.e119866
Scheme 19 MW synthesis of pyrrole by reacting furan-2,5-dione with 3-phenylenediamine.
Coupling microwave photons to a mechanical resonator using quantum interference
<p>This contains the data and processing scripts used for the figures of the manuscript "Coupling microwave photons to a mechanical resonator using quantum interference"</p>
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