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3 results for “Continuous flow synthesis”
Continuous-Flow Synthesis of BiVO4 Nanoparticles: From laboratory scale to practical systems
<p>#Data set of "Continuous-Flow Synthesis of BiVO4 Nanoparticles: From laboratory scale to practical systems"</p> <p>---</p> <p>## GENERAL INFORMATION</p> <p>1. Data set title: "Continuous-Flow Synthesis of BiVO4 Nanoparticles: From laboratory scale to practical systems"</p> <p>2.Authorship: <br> Name: Christian Robles<br> Institution: Institute of Advanced Materials (INAM), Universitat Jaume I, 12006, Castelló, Spain<br> ORCID: 0000-0003-1166-2950</p> <p> Name: Laura Montañés<br> Institution: Institute of Advanced Materials (INAM), Universitat Jaume I, 12006, Castelló, Spain<br> ORCID: 0000-0002-1076-013X <br> <br> Name: Camilo A. Mesa<br> Institution: Institute of Advanced Materials (INAM), Universitat Jaume I, 12006, Castelló, Spain<br> ORCID: 0000-0002-8450-2563</p> <p> Name:Diego Iglesias <br> Institution: institute of Advanced Materials (INAM), Universitat Jaume I, 12006, Castelló, Spain<br> ORCID: 0000-0002-4030-5816</p> <p> Name: Helena Rabelo<br> Institution: Catalan Institute of Nanoscience and Nanotechnology (ICN2) and BIST, Campus UAB, Ballaterra, 08193, Barcelona, Spain<br> ORCID: 0000-0002-7773-3929</p> <p> Name: Maria Chiara Spadaro<br> Institution: Catalan Institute of Nanoscience and Nanotechnology (ICN2) and BIST, Campus UAB, Ballaterra, 08193, Barcelona, Spain. Department SIMAU, Marche Polytechnic University, 60131, Ancona, Italy.<br> ORCID: 0000-0002-6540-0377<br> <br> Name: Jordi Arbiol<br> Institution: Catalan Institute of Nanoscience and Nanotechnology (ICN2) and BIST, Campus UAB, Ballaterra, 08193, Barcelona, Spain ICREA, 08010, Barcelona, Spain<br> ORCID: 0000-0002-0695-1726</p> <p> Name: Jesús Redondo<br> Institution: Department of Polymers and Advanced Materials, Centro de Física de Materiales CFM (UPV/EHU-CSIC), University of the Basque Country UPV/EHU, 20018, San Sebastián Spain. Department of Surface and Plasma Science, Faculty of Mathematics and Physics, Charles University, 180 00 Prague 8, Czech Republic<br> ORCID: 0000-0002-8147-689X</p> <p> Name: F.Schiller<br> Institution: Department of Polymers and Advanced Materials, Centro de Física de Materiales CFM (UPV/EHU-CSIC), University of the Basque Country UPV/EHU, 20018, San Sebastián Spain. Donostia International Physics Center DIPC, 20018 San Sebastián, Spain<br> ORCID: 0000-0003-1727-3542</p> <p> Name:Sara Barja<br> Institution: Department of Polymers and Advanced Materials, Centro de Física de Materiales CFM (UPV/EHU-CSIC), University of the Basque Country UPV/EHU, 20018, San Sebastián Spain. Donostia International Physics Center DIPC, 20018 San Sebastián, Spain. IKERBASQUE, Basque Foundation for Science, 48009 Bilbao, Spain</p> <p> Name: Beatriz Julián-López<br> Institution: Institude of Advanced Materials (INAM), Universitat Jaume I, 12006, Castelló, Spain<br> ORCID: 0000-0003-1019-776X</p> <p> Name: Ana Gutiérrez-Blanco<br> Institution: Institude of Advanced Materials (INAM), Universitat Jaume I, 12006, Castelló, Spain<br> ORCID: 0000-0001-9412-2321<br> Email: <angutier@uji.es></p> <p> Name: Victor Sans<br> Institution: Institude of Advanced Materials (INAM), Universitat Jaume I, 12006, Castelló, Spain<br> ORCID: 0000-0001-7045-5244<br> Email: <sans@uji.es></p> <p> Name: Sixto Giménez<br> Institution: Institude of Advanced Materials (INAM), Universitat Jaume I, 12006, Castelló, Spain<br> ORCID: 0000-0002-4522-3174<br> Email: <sjulia@uji.es></p> <p>## FILE DESCRIPTION<br>----------------<br>### Figure 1<br>-Fig1b.txt : Distribution hystogram of the BiVO4 NPs after the synthetic procedure.</p> <p>### Figure 3 (All measurements were carried out in 0.1 M potassium phosphate buffer (pH 7), containing 0.1 M Na2SO3 as hole scavenger.)<br>-Fig3a.txt : LSVs under chopped illumination conditions, scan rate, 10 mV·s-1, simulated solar light (AM 1.5 G, 100 mW·cm-2), back illumination.<br>-Fig3b.txt : Chronoamperometries at 1.23 V vs. RHE.<br>-Fig3c.txt : IPCE measurements and integrated photocurrent at 1.23 V vs. RHE</p> <p>### Figure 4<br>-Fig4c.txt : LSV of the measured photoanode (the electrolyte consisted on 0.5 M KPi at a constant pH of 7 and 0.5 M Na2SO3 as hole scavenger) with back illumination configuration.</p> <p>### Figure S4<br>-FigS4a.txt : Absorbance spectra of the different BiVO4 colloidal suspension alliquots taken for reproducibility studies.Seven consecutive synthetic runs were carried out and an aliquot was taken from each run, always under identical conditions regarding the collection time of the sample (30 minutes after starting the reaction).<br>-FigS4b.txt : Transmittance spectra of the different BiVO4 colloidal suspension alliquots taken for reproducibility studies.Seven consecutive synthetic runs were carried out and an aliquot was taken from each run, always under identical conditions regarding the collection time of the sample (30 minutes after starting the reaction).<br>-FigS4c.txt : Absorbance mean + error or the different BiVO4 colloidal suspension alliquots taken for reproducibility studies.<br>-FigS4d.txt : Transmittance at the selcted wavelength (400 nm) for the different BiVO4 colloidal suspension alliquots taken for reproducibility studies.</p> <p>## Figure S6<br>-FigS6.txt : Thermogravimetric analysis (TGA) curve of the BiVO4 NPs from room temperature to 500 ºC.</p> <p>### Figure S7<br>-FigS7.txt : XRD patterns of the FTO/BiVO4 photoanodes before and after thermal annealing. </p> <p>### Figure S8<br>-FigS8a.txt : Raman spectra of the FTO/BiVO4/Al2O3 based films before and after annealing. <br>-FigS8b.txt : FT-IR spectra of the FTO/BiVO4/Al2O3 based films before and after annealing. </p> <p>### Figure S9<br>-FigS9a.txt : Absorptance spectra of the FTO/BiVO4/Al2O3 samples before and after the annealing process.<br>-FigS9b.txt : Tauc plot of the FTO/BiVO4/Al2O3 samples before and after the annealing process. </p> <p>### Figure S11<br>-Fig11a.txt : LSV of the FTO/BiVO4/Al2O3 films in 0.1 M potassium phosphate buffer (pH 7) containing 0.1 M Na2SO3 as hole scavenger under AM 1.5 G, 100 mW·cm-2 back side illumination (scan rate, 10 mV·s-1) for the deposition reproducibility studies.<br>-Fig11b takes the same data contained in Fig11a.txt</p> <p>### Figure S12 (Measurements in 0.1 M phosphate buffer (pH 7) containing 0.1 M Na2SO3 as hole scavenger under AM 1.5 G, 100 mW·cm-2 back side illumination.)<br>-FigS12a.txt : Consecutive LSVs (LSV1, LSV2 LSV3) and LSV after 2 hours testing for the FTO/BiVO4 (area 5 cm2).<br>-FigS12b.txt : Consecutive LSVs (LSV1, LSV2 LSV3) and LSV after 2 hours testing for the FTO/BiVO4/Al2O3 films (area 5 cm2) showing the enhanced stability after deposition of the Al2O3 layer.</p> <p> </p>
Continuous Flow Synthesis of Iron Oxide Nanoparticles Using Water-in-Oil Microemulsion_experimental_dataset
<p>This dataset contains the raw experimental data to the article Sopoušek et al., Continuous Flow Synthesis of Iron Oxide Nanoparticles<br> Using Water-in-Oil Microemulsion, Colloid Journal, 2020, Vol. 82, No. 6, pp. 727–734. </p>
Continuous Flow Synthesis and Simulation-Supported Investigation of Tunable Plasmonic Gold Patchy Nanoparticles
<p>This is the dataset for the following manuscript "Continuous Flow Synthesis and Simulation-Supported Investigation of Tunable Plasmonic Gold Patchy Nanoparticles".</p> <p>Abstract</p> <p><span>Plasmonic nanoparticles have intriguing optical properties which make them suitable candidates for sensing or theranostic applications. Anisotropic patchy particles, where metal is locally deposited on the surface of a core particle, exhibit plasmon resonances that can be specifically adjusted for these applications. However, many existing synthesis routes are complex, yield too little material, or provide particles with limited optical tunability. In this work, we present a simple and scalable continuous flow synthesis of gold-on-polystyrene patchy particles with widely adjustable optical properties. By increasing the chloride concentration in the electroless deposition of gold, we slow down the redox reduction kinetics and obtain a dense patch morphology as well as a reduced nucleation rate. The latter is counteracted by introducing a low-level seeding approach where a small number of gold nanocrystals heterocoagulate with the core particles prior to patch growth. Seeding and patch growth are performed in a continuous flow set-up with two T-shaped milli-mixers. The resulting patchy particle samples exhibit a tunable dipolar plasmon peak between 600 nm and 1100 nm. We also investigate the structure-property relationship for our gold patchy particles using Finite Element Method simulations. After identifying a suitable patch shape model, we elucidate the influence of individual geometric parameters on the optical properties and show that the relationship holds true for a large range of patch coverages. Finally, we apply the relationship to explain the time-dependent change in the optical properties of as-synthesized patches by correlating it with the patch shape transformation revealed by electron microscopy.</span></p> <p> </p> <p>The uploaded data are sorted by figure.</p>
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