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7 results for “crystallization kinetics”
Datasets supporting the publication "Technical Note: in-situ measurements and modelling of the oxidation kinetics in films of a cooking aerosol proxy using a Quartz Crystal Microbalance with Dissipation monitoring (QCM-D)" by Milsom et al.
<p>Supporting experimental and modelling data for the manuscript entitled "Technical Note: Modelling and in-situ measurements of the oxidation kinetics in films of a cooking aerosol proxy using a Quartz Crystal Microbalance with Dissipation monitoring (QCM-D)" by Adam Milsom et al. 2023. </p> <p>Includes raw QCM-D data with the numbers at the beginning of the files corresponding to the experiment numbers in the manuscript. </p> <p>Normalised Raman peak area data for modelling and model ensemble outputs, including uptake coefficients. </p>
A synchrotron X-ray scattering study of the crystallization behavior of mixtures of confectionary triacylglycerides: effect of chemical composition and shear on polymorphism and kinetics
<p>Processed and raw data associated at the publication: <a href="https://www.sciencedirect.com/science/article/pii/S0963996923014126" target="_blank" rel="noopener">A synchrotron X-ray scattering study of the crystallization behavior of mixtures of confectionary triacylglycerides: effect of chemical composition and shear on polymorphism and kinetics - ScienceDirect</a></p>
Removal of Crystal Violet (CV) in aqueous solution by Activated Carbon- Equilibrium, kinetic and Thermodynamic
<p>The quantitative kinetic and equilibrium adsorption parameters for Crystal Violet (CV) removed by commercial activated carbon (AC) were studied by UV visible absorption spectroscopy. (AC) with a high specific surface area (1250.320m2 /g) was characterized by the Brunauer-Emmett-Teller (BET) method and the zero charge point (pzc).The adsorptive properties of (AC) with (CV) was conducted at variable stirring speed , adsorbent dose, solution pH, initial (CV) concentrations, contact time and temperature using batch mode operation to find the optimal conditions for a maximum adsorption. The adsorption mechanism of CV onto (AC) was studied using the first pseudo order, second pseudo order and Elovich kinetic models. The kinetic was found to follow a pseudo-second order kinetic model. The equilibrium adsorption data for CV on AC were analyzed by the Langmuir, Freundlich, Elovich and Temkin models. The results indicate that the Langmuir model provides the best correlation (qmax = 35.71, 90.91 mg/g at 25 °C and 40 °C respectively).The adsorption isotherms at different temperatures have been used for the determination of thermodynamic parameters i.e. the free energy (ΔGo = -2.30 to -5.34 kJ/mol), enthalpy (ΔHo = 36.966 kJ/mol), entropy (ΔSo = 0.131 kJ/mol K) and activation energy (Ea) 40.208 kJ/mol of adsorption. The negative ΔGo and positive ΔHo values indicate that the overall adsorption is spontaneous and endothermic in nature</p>
Liquid-liquid phase reaction between crystal violet and sodium hydroxide: kinetic study and precipitate analysis
<p>To investigate reaction order and kinetic parameters of the reaction between crystal violet (CV) and sodium hydroxide (NaOH), various concentrations of the reactants were applied. The present work also verifies the unknown solid product produced under highly concentrated conditions. The reaction orders of CV and NaOH were determined to be 1 and 1.17 by pseudo-rate method, respectively, with a rate constant, k, of 0.084 [(M-1.17) s-1]. In addition to pseudo-rate method, the half-life approach is use to calculated the overall reaction order to verify the accuracy of pseudo-rate method. The overall reaction order is determined to be 1.9 by half-life method. Compare reaction order gained from both methods, the overall reaction order is determined as ~2. The precipitate formation was observed when high concentrations of CV (0.01~0.1 M) and NaOH (1.0 M) were applied. Fourier transform infrared (FTIR) spectroscopy was used to compare the spectra of the precipitate generated and a commercial solvent violet 9 (SV9). Based on the FTIR spectra, it was confirmed that the molecular structure of the precipitate matched that of solvent violet 9.</p>
Liquid-liquid phase reaction between crystal violet and sodium hydroxide: kinetic study and precipitate analysis
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In Situ Probing the Crystallization Kinetics in Gas-Quenching-Assisted Coating of Perovskite Films
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Data and materials for "Crystallization kinetics of atomic crystals revealed by a single-shot and single-particle X-ray diffraction experiment"
<p>XFEL diffraction data and simulation codes associated with publication "Crystallization kinetics of atomic crystals revealed by a single-shot and single-particle X-ray diffraction experiment" (https://doi.org/10.1073/pnas.2111747118). <a href="https://zenodo.org/api/files/6b7e2270-da94-43ea-8cb7-24db901d6d47/Fig1A.txt?versionId=22020722-9489-427b-b2a3-8a5577542679">Fig1A.txt</a> is the 2D array data of the accumulated diffraction image. <a href="https://zenodo.org/api/files/6b7e2270-da94-43ea-8cb7-24db901d6d47/Fig2A.txt?versionId=f53f0a51-20f0-4aaa-b2f3-7ac284e5a39a">Fig2A.txt</a>, <a href="https://zenodo.org/api/files/6b7e2270-da94-43ea-8cb7-24db901d6d47/Fig2B.txt?versionId=a7a31743-446f-4b60-84fc-8d06383bd852">Fig2B.txt</a>, <a href="https://zenodo.org/api/files/6b7e2270-da94-43ea-8cb7-24db901d6d47/Fig2C.txt?versionId=d79d2068-2530-4ee6-95fc-b38b4ee8bda5">Fig2C.txt</a> are the 2D arrays of the single-shot diffraction images. The unit is electronvolt per pixel. <a href="https://zenodo.org/api/files/6b7e2270-da94-43ea-8cb7-24db901d6d47/Python%20script.ipynb">Python script.ipynb</a> includes the simulation codes for the single-shot streak patterns and the integrated powder diffraction pattern. </p>
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