3DED data collected on CAU-42 (April/May 2017)

<p>Datasets were collected on a 200 kV JEOL 2100 LaB6 transmission electron microscope at the Department of Materials and Environmental Chemistry, Stockholm University. The detector was a 512x512 pixel TimePix detector controlled through SoPhy, the software supplied with the detector.</p> <p>The crystal was manually moved to stay within the aperture when needed based on the intensity of the diffraction pattern. Data collection and previous processing are further described in Leubner et al., Dalton Trans., 2020, 49, 3088&ndash;3092 (DOI: 10.1039/d0dt00235f). The data used for structure determination in the paper are found in the folder 170517/1/SMV.</p> <p>Diffraction patterns in TIFF format are the original. A conversion script was used to convert the TIFF images to SMV format.</p> <p>The sample was cooled to liquid nitrogen temperature (98 K) during data collection.</p>