Natrolite - Sample 2 NanED Round Robin, Data: ESR8 & ESR9

<p><em><strong>Natrolite</strong></em></p> <p>The following submission contains the data collection and processing for the sample natrolite under the NanEd round-robin project.&nbsp; Precession Electron Diffraction (PED) was&nbsp;used to collect the dataset&nbsp;on the target&nbsp;crystal.&nbsp; The dataset&nbsp;was&nbsp;processed with PETS2 and eADT software. The table below summarizes the data collection parameters for the dataset.</p> <p>&nbsp;</p> <table> <tbody> <tr> <td> <p><strong>General information:</strong></p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>Project</p> </td> <td> <p>NanED (www.naned.eu)</p> </td> </tr> <tr> <td> <p>ESR Project</p> </td> <td> <p>ESR8 &amp; ESR9 - Round Robin</p> </td> </tr> <tr> <td> <p>Project Label</p> </td> <td> <p>RR2</p> </td> </tr> <tr> <td> <p>Sample Label</p> </td> <td> <p>RR2-S2_ PRAHA</p> </td> </tr> <tr> <td> <p>Data set Label</p> </td> <td> <p>RR2_Cry2</p> </td> </tr> <tr> <td> <p>&nbsp;</p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p><strong>Instrumental:</strong></p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>Instrument</p> </td> <td> <p>FEI TECNAI F30 STWIN</p> </td> </tr> <tr> <td> <p>Radiation source</p> </td> <td> <p>FEG</p> </td> </tr> <tr> <td> <p>Accelerating voltage</p> </td> <td> <p>300 kV</p> </td> </tr> <tr> <td> <p>Wavelength</p> </td> <td> <p>0.0197 &Aring;</p> </td> </tr> <tr> <td> <p>Probe Type</p> </td> <td> <p>Nanodiffraction</p> </td> </tr> <tr> <td> <p>Beam Diameter</p> </td> <td> <p>200nm</p> </td> </tr> <tr> <td> <p>Beam Convergence</p> </td> <td> <p>Semi-parallel beam</p> </td> </tr> <tr> <td> <p>Detector</p> </td> <td> <p>US4000 - CCD camera GATAN (16-bit) (bottom mounted)</p> </td> </tr> <tr> <td> <p>Number of pixels in the image</p> </td> <td> <p>2048 x 2048</p> </td> </tr> <tr> <td> <p>Pixel size</p> </td> <td> <p>15 &micro;m x 15 &micro;m</p> </td> </tr> <tr> <td> <p>Camera Length / Effective Camera Length</p> </td> <td> <p>750 mm / 702 mm</p> </td> </tr> <tr> <td> <p>Calibration constant (not corrected for Effective Camera length)</p> </td> <td> <p>0.00152 &Aring;^-1/pixel</p> </td> </tr> <tr> <td> <p>&nbsp;Hardware Binning</p> </td> <td> <p>2&nbsp;</p> </td> </tr> <tr> <td> <p><strong>Sample description:</strong></p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>Name</p> </td> <td> <p>Natrolite</p> </td> </tr> <tr> <td> <p>Chemical composition</p> </td> <td> <p>Na₂Al₂Si₃O₁₀&middot;2H₂O</p> </td> </tr> <tr> <td> <p>Sample source</p> </td> <td> <p>Natural sample from Marianska Skala, Usti nad Labem, Czechia</p> </td> </tr> <tr> <td> <p>Sample preparation</p> </td> <td> <p>The crystals were grinded in an agata mortar and part of the resulting powder was loaded on the carbon side of a carbon-coated copper grid (300 mesh).</p> </td> </tr> <tr> <td> <p><strong>Experimental:</strong></p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>Data Type</p> </td> <td> <p>Electron diffraction data - 3D ED</p> </td> </tr> <tr> <td> <p>Data collection method</p> </td> <td> <p>Precession</p> </td> </tr> <tr> <td> <p>Temperature (K) used during data collection</p> </td> <td> <p>293 K</p> </td> </tr> <tr> <td> <p>Number of crystals contributing to the data set</p> </td> <td> <p>1</p> </td> </tr> <tr> <td> <p>Number of experimental frames</p> </td> <td> <p>131</p> </td> </tr> <tr> <td> <p>tilt range, tilt step, tilt per frame</p> </td> <td> <p>-65&deg; to +65&deg;, 1&deg;, 0&deg;</p> </td> </tr> <tr> <td> <p>Precession angle</p> </td> <td> <p>1&deg;</p> </td> </tr> <tr> <td> <p>Exposure time per frame</p> </td> <td> <p>250 ms</p> </td> </tr> <tr> <td> <p>&nbsp;</p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p><strong>Software:</strong></p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>Software used for the data collection</p> </td> <td> <p>Gatan Digital Micrograph software</p> </td> </tr> <tr> <td> <p>Software used for processing</p> </td> <td> <p>PETS2 and eADT</p> </td> </tr> <tr> <td> <p>&nbsp;</p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p><strong>Authorship and bibliography</strong></p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>Author(s) of the data</p> </td> <td> <p>Laura Gemmrich Hern&aacute;ndez (ESR8) &amp; Marco Santucci (ESR9)</p> </td> </tr> <tr> <td> <p>Related data</p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>Publication(s)</p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>&nbsp;</p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p><strong>Files and data formats</strong></p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>Image folder</p> </td> <td> <p>img: Folder containing images of the diffraction pattern from each frame.</p> </td> </tr> <tr> <td> <p>Image format</p> </td> <td> <p>tiff_16bit_unsigned</p> </td> </tr> <tr> <td> <p>&nbsp;</p> </td> <td> <p>&nbsp;</p> </td> </tr> </tbody> </table> <p>&nbsp;</p> <p>&nbsp;</p> <p>&nbsp;</p>