Epidote - Sample 1 NanED Round Robin, Data ESR3

<table> <tbody> <tr> <td> <p><strong>General information:</strong></p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>Project</p> </td> <td> <p>NanED (www.naned.eu)</p> </td> </tr> <tr> <td> <p>ESR Project</p> </td> <td> <p>ESR3</p> </td> </tr> <tr> <td> <p>&nbsp;</p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p><strong>Instrumental:</strong></p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>Instrument</p> </td> <td> <p>FEI TECNAI</p> </td> </tr> <tr> <td> <p>Radiation source</p> </td> <td> <p>FEG</p> </td> </tr> <tr> <td> <p>Accelerating voltage</p> </td> <td> <p>200 kV</p> </td> </tr> <tr> <td> <p>Wavelength</p> </td> <td> <p>0.0251 &Aring;</p> </td> </tr> <tr> <td> <p>Acquisiton Method</p> </td> <td> <p>SAED</p> </td> </tr> <tr> <td> <p>Detector</p> </td> <td> <p>Eagle &ndash; CCD Camera</p> </td> </tr> <tr> <td> <p>Number of pixels in the image</p> </td> <td> <p>2048 x 2048</p> </td> </tr> <tr> <td> <p>Calibration constant (not corrected for Effective Camera length)</p> </td> <td> <p>0.00182 &Aring;^-1/pixel</p> </td> </tr> <tr> <td> <p><strong>Sample description:</strong></p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>Name</p> </td> <td> <p>Epidote</p> </td> </tr> <tr> <td> <p>Chemical composition</p> </td> <td> <p>Ca2FexAl3-xSi3O13H</p> </td> </tr> <tr> <td>&nbsp;</td> <td>&nbsp;</td> </tr> <tr> <td> <p><strong>Experimental:</strong></p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>Data Type</p> </td> <td> <p>Electron diffraction data - 3D ED</p> </td> </tr> <tr> <td> <p>Data collection method</p> </td> <td> <p>Stepwise</p> </td> </tr> <tr> <td> <p>Temperature (K) used during data collection</p> </td> <td> <p>293 K</p> </td> </tr> <tr> <td> <p>Number of crystals contributing to the data set</p> </td> <td> <p>1</p> </td> </tr> <tr> <td> <p>Number of experimental frames</p> </td> <td> <p>351</p> </td> </tr> <tr> <td> <p>tilt range, tilt step</p> </td> <td> <p>-35&deg; to +35&deg;, 0.2&deg;</p> </td> </tr> <tr> <td> <p>Exposure time per frame</p> </td> <td> <p>1s</p> </td> </tr> <tr> <td> <p>&nbsp;</p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p><strong>Software:</strong></p> </td> <td> <p>&nbsp;</p> </td> </tr> <tr> <td> <p>Software used for the data collection</p> </td> <td> <p>TIA</p> </td> </tr> <tr> <td> <p>Software used for processing</p> </td> <td> <p>PETS2</p> </td> </tr> <tr> <td> <p>Software used for Solution</p> </td> <td> <p>Jana</p> </td> </tr> <tr> <td> <p>Software used for refinement</p> </td> <td> <p>Olex2</p> </td> </tr> </tbody> </table>