Enantiopure Ibuprofen - Sample 3 NanED, Data ESR1 & ESR2

<strong>General Information</strong> &nbsp; Project NanED (www.naned.eu) ESR Project ESR1 &amp; ESR2 <strong>Instrumental</strong> &nbsp; Instrument Zeiss Libra 120 Radiation source LaB6 Accelerating voltage 120 kV Wavelength 0.0335&nbsp;&Aring; Probe Type Nanodiffraction Beam Diameter 600 nm Beam Convergence Parallel beam Detector Timepix Single Electron Detector Number of pixels in the image 512 x 512 Physical pixel size 55&nbsp;&micro;m * 55&nbsp;&micro;m Effective camera length 180 mm Calibration constant 0.004815 &Aring;^-1/pixel &nbsp; &nbsp; <strong>Sample description</strong> &nbsp; Name Ibuprofen Chemical composition C₁₃H₁₈O₂ Sample source Thermo Scientific (catalog. No: 333200050, lot: A0424385) Sample preparation Crushed between two glass slides &nbsp; &nbsp; <strong>Experimental</strong> &nbsp; Data type 3D Electron Diffraction (3D-ED) Data collection method Continuous Rotation Electron Diffraction (CRED) Rotation Speed 1.125 &ordm;/s Temperature 95.15 K Number of crystals contributing to the dataset 1 Number of experimental frames 226 Tilt range, tilt step -60&ordm; to +55, 0.5&ordm; Exposure time per frame 450 ms &nbsp; &nbsp; <strong>Software</strong> &nbsp; Software used for data collection WinTEM (Zeiss), Digistar (NanoMEGAS) and Sophy (Software for Physics) Software used for processing Pets2 Software used for solution Shelxt Software used for refinement Jana, Olex2 &nbsp; &nbsp; <strong>Authorship and bibliography</strong> &nbsp; Author(s) of the data Moussa Diame FAYE (ESR1) &amp; Vincentia Emerson Agbemeh (ESR2) Related data &nbsp; Publication(s) &nbsp; &nbsp; &nbsp; <p>&nbsp;</p> <p><strong>Precession:</strong></p> <strong>General Information</strong> &nbsp; Project NanED (www.naned.eu) ESR Project ESR1 &amp; ESR2 <strong>Instrumental</strong> &nbsp; Instrument Zeiss Libra 120 Radiation source LaB6 Accelerating voltage 120 kV Wavelength 0.0335&nbsp;&Aring; Probe Type Nanodiffraction Beam Diameter 150 nm Beam Convergence Parallel beam Detector Timepix Single Electron Detector Number of pixels in the image 512 x 512 Physical pixel size 55&nbsp;&micro;m * 55&nbsp;&micro;m Effective camera length 180 mm Calibration constant 0.004815 &Aring;^-1/pixel &nbsp; &nbsp; <strong>Sample description</strong> &nbsp; Name Ibuprofen Chemical composition C₁₃H₁₈O₂ Sample source Thermo Scientific (catalog. No: 333200050, lot: A0424385) Sample preparation Crushed between two glass slides &nbsp; &nbsp; <strong>Experimental</strong> &nbsp; Data type 3D Electron Diffraction (3D-ED) Data collection method Precession Precession Semiangle 1&ordm;&nbsp;&nbsp; Temperature 95.15 K Number of crystals contributing to the dataset 1 Number of experimental frames 104 Tilt range, tilt step -60 to +55, 1&ordm; Exposure time per frame 1000 ms &nbsp; &nbsp; <strong>Software</strong> &nbsp; Software used for data collection WinTEM (Zeiss), Digistar (NanoMEGAS) and Sophy (Software for Physics) Software used for processing PETS2 Software used for solution Shelxt Software used for refinement Jana &nbsp; &nbsp; <strong>Authorship and bibliography</strong> &nbsp; Author(s) of the data Moussa Diame FAYE (ESR1) &amp; Vincentia Emerson Agbemeh (ESR2) Related data &nbsp; Publication(s) &nbsp; &nbsp; &nbsp;