In Crystallo Lattice Adaptivity Triggered by Solid-Gas Reactions of Cationic Group 7 Pincer Complexes

<p>3DED/microED datasets of&nbsp;[Mn(ⁱPr-PONOP)(CO)₃][BAr^F₄] collected using a Thermo Fisher Scientific Glacios microscope equipped with a Ceta-D Camera associated with the publication &quot;In Crystallo Lattice Adaptivity Triggered by Solid-Gas Reactions of Cationic Group 7 Pincer Complexes&quot; published in&nbsp;Chem. Commun.</p> <p>Data collection details:</p> <p>200kV, nanoprobe, gun lens 8, spot size 11, 30 &micro;m C2 aperture. Illuminated area was ~1 &micro;m. Under these conditions flux is 0.06 &ndash; 0.07 e-/&Aring;^2/s. Camera length calibrated from Al powder was 958.5 mm. Data acquired using EPU-D with following settings: 2x binning, 2&deg;/s, 0.5s exposure, rolling shutter, noise reduction mode enabled.&nbsp;</p> <p>MRC format images can be processed with DIALS using the FormatMRC dxtbx format (distributed with DIALS from version 3.5 onwards), use goniometer.axes=1,0,0.&nbsp;</p> <p>&nbsp;</p>