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52 results for “Aplysina”
NMR and MS data of identified bromotyrosine alkaloids produced and released by Aplysina cavernicola
<p>This folder contains NMR and MS datasets of each identified bromotyrosine spiroisoxazoline pertaining to the publication<em> </em>entitled:</p> <p><strong>Diving into the molecular diversity of <em>Aplysina cavernicola’s </em>exo-metabolites: contribution of bromo-spiroisoxazoline alkaloids.</strong> <em>ACS Omega</em> 2022 <strong> <a href="https://pubs.acs.org/doi/10.1021/acsomega.2c05415"> </a></strong><a href="https://pubs.acs.org/doi/10.1021/acsomega.2c05415">https://doi.org/10.1021/acsomega.2c05415</a></p> <ul> <li>All NMR data were acquired in CD<sub>3</sub>OD at 600 MHz (Bruker Avance III, cryosonde TCI) using 2 mm NMR tubes</li> <li>All MS<sup>2</sup> data were acquired on a Bruker Impact II qTOF (ESI positive, collision energy 20-40eV)</li> </ul> <p>The compressed folder of the newly described Aplysine1 contains also raw data related to circular dichroism (CD) and infrared (IR) analyses, as well as quantum mechanical calculations of <sup>13</sup>C NMR shifts using GIAO NMR and DP4+ analyses.</p> <p>The Excel spreadsheet for DP4+ analyses were obtained from: Grimblat N et al. “Beyond DP4: An Improved Probability for the Stereochemical Assignment of Isomeric Compounds Using Quantum Chemical Calculations of NMR Shifts.” <em>The Journal of Organic Chemistry</em> 80, no. 24 (December 18, 2015): 12526–34. <a href="https://doi.org/10.1021/acs.joc.5b02396">https://doi.org/10.1021/acs.joc.5b02396</a>.</p> <p>All MS data are also made Freely available at the UCSD Center for Computational Mass Spectrometry database with the MassIVE identifier <a href="https://massive.ucsd.edu/ProteoSAFe/dataset.jsp?task=4f6d3c00539a412a9c6d7fac0f7f2a81">MSV000089502</a> .</p> <p>NOTE: 3,5 dibromotyrosine was not identified neither in<em> Aplysina cavernicola </em>crude extract nor as exo-metabolites but was used for MS dereplication purposes.</p>
Fig. 8 in Three new species of Spongiopsyllus Johnsson, 2000 (Copepoda: Siphonostomatoida: Entomolepididae) associated with Aplysina cauliformis (Carter, 1882) (Porifera: Demospongiae) from Todos-os-Santos Bay, Northeastern Brazil
Fig. 8. Spongiopsyllus aramisi sp. nov., ♀, paratype (UFBA 3300). A. L1. B. L2. C. L3. D. L4. Scale bars = 50 µm.
Fig. 7 in Three new species of Spongiopsyllus Johnsson, 2000 (Copepoda: Siphonostomatoida: Entomolepididae) associated with Aplysina cauliformis (Carter, 1882) (Porifera: Demospongiae) from Todos-os-Santos Bay, Northeastern Brazil
Fig. 7. Spongiopsyllus aramisi sp. nov., ♀, paratype (UFBA 3299). A. Antennule. B. Antenna. C. Stylet. D. Mandibular palp. E. Maxillule. F. Maxilla. G. Maxilliped. Scale bars: A–E = 25 µm; F–G = 50 µm.
Fig. 4 in Three new species of Spongiopsyllus Johnsson, 2000 (Copepoda: Siphonostomatoida: Entomolepididae) associated with Aplysina cauliformis (Carter, 1882) (Porifera: Demospongiae) from Todos-os-Santos Bay, Northeastern Brazil
Fig. 4. Spongiopsyllus porthosi sp. nov., ♀, holotype (UFBA 3292). A. Maxilliped. B. L1. C. L2. D. L3. E. L4. Scale bars = 50 µm.
Fig. 3 in Three new species of Spongiopsyllus Johnsson, 2000 (Copepoda: Siphonostomatoida: Entomolepididae) associated with Aplysina cauliformis (Carter, 1882) (Porifera: Demospongiae) from Todos-os-Santos Bay, Northeastern Brazil
Fig. 3. Spongiopsyllus porthosi sp. nov., ♀, holotype (UFBA 3292). A. Habitus, dorsal view. B. Urosome. C. Antennule. D. Antenna. E. Mandibular palp. F. Maxillule. G. Maxilla. Scale bars: A = 200 µm; B = 50 µm; C–F = 25 µm; G = 50 µm.
Fig. 6 in Three new species of Spongiopsyllus Johnsson, 2000 (Copepoda: Siphonostomatoida: Entomolepididae) associated with Aplysina cauliformis (Carter, 1882) (Porifera: Demospongiae) from Todos-os-Santos Bay, Northeastern Brazil
Fig. 6. Spongiopsyllus aramisi sp. nov., ♀, paratype (UFBA 3299). A. Habitus, dorsal view. B. Urosome. Scale bars: A = 200 µm; B = 100 µm.
Fig. 5 in Three new species of Spongiopsyllus Johnsson, 2000 (Copepoda: Siphonostomatoida: Entomolepididae) associated with Aplysina cauliformis (Carter, 1882) (Porifera: Demospongiae) from Todos-os-Santos Bay, Northeastern Brazil
Fig. 5. Spongiopsyllus porthosi sp. nov., ♂, allotype (UFBA 3293). A. Habitus, dorsal view. B. Urosome. C. Antennule. Scale bars: A = 100 µm; B–C = 25 µm.
Fig. 2 in Three new species of Spongiopsyllus Johnsson, 2000 (Copepoda: Siphonostomatoida: Entomolepididae) associated with Aplysina cauliformis (Carter, 1882) (Porifera: Demospongiae) from Todos-os-Santos Bay, Northeastern Brazil
Fig. 2. Spongiopsyllus athosi sp. nov., ♀, holotype (UFBA 3291). A. Maxilliped. B. L1. C. L2. D. L3. E. L4. Scale bars = 50 µm.
Fig. 1 in Three new species of Spongiopsyllus Johnsson, 2000 (Copepoda: Siphonostomatoida: Entomolepididae) associated with Aplysina cauliformis (Carter, 1882) (Porifera: Demospongiae) from Todos-os-Santos Bay, Northeastern Brazil
Fig. 1. Spongiopsyllus athosi sp. nov., ♀, holotype (UFBA 3291). A. Habitus, dorsal view. B. Urosome. C. Antennule. D. Antenna. E. Mandibular palp. F. Maxillule. G. Maxilla. Scale bars: A = 200 µm; B–G = 50 µm.
Table 4 in Three new species of Spongiopsyllus Johnsson, 2000 (Copepoda: Siphonostomatoida: Entomolepididae) associated with Aplysina cauliformis (Carter, 1882) (Porifera: Demospongiae) from Todos-os-Santos Bay, Northeastern Brazil
<p><b>Table 4.</b> Comparison of species of <i>Spongiopsyllus</i> Johnsson, 2000.</p><table><tbody><tr><th></th><th><b>A1</b></th><th><b>A1</b></th><th><b>A1</b></th><th><b>A2</b></th><th><b>A2</b></th><th><b>A2</b></th><th><b>Mxll</b></th><th><b>Mxll</b></th><th><b>Mxlp</b></th></tr></tbody><tbody><tr><th></th><td><b>nº of segments</b></td><td><b>aesthetasc segment</b></td><td><b>fused segments</b></td><td><b>nº of exopod spinules</b></td><td><b>nº of segment endopod</b></td><td><b>nº of setae on 2</b> <b>nd</b> <b>endopod</b></td><td><b>nº of setae on inner lobe</b></td><td><b>nº of setae on outer lobe</b></td><td><b>endopod formula</b></td></tr><tr><th><i>S. adventici</i> us Johnsson, 2000</th><td>17</td><td>15</td><td>III–V, VII–VIII, IX–XII, XXII– XXIII, XXIV– XXVIII</td><td>4</td><td>3</td><td>1 short</td><td>3</td><td>3</td><td>0,2,1+claw</td></tr><tr><th><i>S. redactus</i> Canário <i>et al</i>., 2012</th><td>15</td><td>14</td><td>II–III, IV–VI, IX–XIII, XXII–XX- VIII</td><td>3</td><td>2</td><td>1 long 2 short</td><td>3</td><td>3</td><td>2,1,1+claw</td></tr><tr><th><i>S. atypicus</i> Canário <i>et al</i>., 2019</th><td>14</td><td>12</td><td>III–VIII, IX–XIII, XXII– XXIII, XIV– XVIII</td><td>7</td><td>2</td><td>2 long 2 short</td><td>4</td><td>4</td><td>2,0,1+claw</td></tr><tr><th><i>S. intermedius</i> Borges <i>et al</i>., 2021</th><td>16</td><td>14</td><td>II–III, IV–VI, IX–XIII, XXIII– XXVIII</td><td>5</td><td>2</td><td>1 long 1 short</td><td>2</td><td>3</td><td>1,1,1+claw</td></tr><tr><th><i>S. athosi</i> sp. nov.</th><td>16</td><td>14</td><td>III–VI, IX–XIII, XXIII– XXVIII</td><td>5</td><td>2</td><td>2 long 2 short</td><td>3</td><td>4</td><td>2,1,1+claw</td></tr><tr><th><i>S. porthosi</i> sp.nov.</th><td>16</td><td>14</td><td>III–VI, IX–XIII, XXIII– XXVIII</td><td>5</td><td>2</td><td>2 long 2 short</td><td>4</td><td>4</td><td>2,2,0+claw</td></tr><tr><th><i>S. aramisi</i> sp. nov.</th><td>16</td><td>14</td><td>III–VI, IX–XIII, XXIII– XXVIII</td><td>6</td><td>2</td><td>1 long 1 short</td><td>4</td><td>4</td><td>2,1,1+claw</td></tr></tbody></table>
Table 3 in Three new species of Spongiopsyllus Johnsson, 2000 (Copepoda: Siphonostomatoida: Entomolepididae) associated with Aplysina cauliformis (Carter, 1882) (Porifera: Demospongiae) from Todos-os-Santos Bay, Northeastern Brazil
<p><b>Table 3.</b> <i>Spongiopsyllus aramisi</i> sp.nov., armature formula of L1–L4.</p><table><tbody><tr><th></th><th><b>coxa</b></th><th><b>basis</b></th><th><b>exopod</b></th><th><b>endopod</b></th></tr></tbody><tbody><tr><th><b>L1</b></th><td>0-0</td><td>1-1</td><td>I-1; I-1; II,I,4</td><td>0-1; 0-2; 1,5</td></tr><tr><th><b>L2</b></th><td>0-1</td><td>1-0</td><td>I-1; I-1; III,I,4</td><td>0-1; 0-2; 1,2,2</td></tr><tr><th><b>L3</b></th><td>0-0</td><td>0-0</td><td>I-1; I-1; II,I,4</td><td>0-0; 0-1; 0,1,1</td></tr><tr><th><b>L4</b></th><td></td><td>0-0</td><td>I-0; I-1; II,I,3</td><td>absent</td></tr></tbody></table>
Table 1 in Three new species of Spongiopsyllus Johnsson, 2000 (Copepoda: Siphonostomatoida: Entomolepididae) associated with Aplysina cauliformis (Carter, 1882) (Porifera: Demospongiae) from Todos-os-Santos Bay, Northeastern Brazil
<p><b>Table 1.</b> <i>Spongiopsyllus athosi</i> sp.nov., armature formula of L1–L4.</p><table><tbody><tr><th></th><th><b>coxa</b></th><th><b>basis</b></th><th><b>exopod</b></th><th><b>endopod</b></th></tr></tbody><tbody><tr><th><b>L1</b></th><td>0-1</td><td>0-1</td><td>I-1; I-1; III,3</td><td>0-1; 0-2; 1,5</td></tr><tr><th><b>L2 L3 L4</b></th><td>0-1 0-0 0-0</td><td>0-0 0-0 0-0</td><td>I-1; I-1; III,I,4 I-1; I-1; II,I,4 I-1; I-0; II,I,3</td><td>0-1; 0-2; 1,2,2 0-0; 0-1; 0,1,1 absent</td></tr><tr><th><b>L1</b></th><td>0-1</td><td>1-1</td><td>I-1; I-1; III,4</td><td>0-1; 0-1; 1,5</td></tr><tr><th><b>L2</b></th><td>0-1</td><td>1-0</td><td>I-1; I-1; III,I,4</td><td>0-1; 0-2; 1,2,2</td></tr><tr><th><b>L3</b></th><td>0-0</td><td>0-0</td><td>I-1; I-1; II,I,4</td><td>0-0; 0-1; 0,1,1</td></tr><tr><th><b>L4</b></th><td>0-0</td><td>0-0</td><td>I-1; I-1; II,I,3</td><td>absent</td></tr></tbody></table>
FIGURE 22 in Aplysina Nardo (Porifera, Verongida, Aplysinidae) from the Brazilian coast with description of eight new species
FIGURE 22: Map showing the distribution of Aplysina along the Brazilian coastline. A. Aplysina orthoreticulata sp.n. B. Aplysina pseudolacunosa sp.n. C. Aplysina solangeae sp.n.. Scale bar = 500 km.
FIGURE 21 in Aplysina Nardo (Porifera, Verongida, Aplysinidae) from the Brazilian coast with description of eight new species
FIGURE 21: A–C. Aplysina orthoreticulata sp.n.—Holotype. (MNRJ 4651) A. habit after preservation. B. Skeletal architecture. C. Spongin fibres. Scale bars = A. 1 cm, B. 500 µm, C. 50 µm.
FIGURE 18 in Aplysina Nardo (Porifera, Verongida, Aplysinidae) from the Brazilian coast with description of eight new species
FIGURE 18: A–D. Aplysina lactuca sp.n. Holotype (MNRJ 5477). A–B. habit after preservation. C. Skeletal architecture. D. Spongin fibres. Scale bars = A–B. 5 cm, C. 500 µm, D. 50 µm.
FIGURE 15 in Aplysina Nardo (Porifera, Verongida, Aplysinidae) from the Brazilian coast with description of eight new species
FIGURE 15: A–D. Aplysina cristagallus sp.n. Holotype (MNRJ 3528). A–B. habit after preservation. C. Skeletal architecture. D. Spongin fibres. Scale bars = A–B. 1 cm, C. 500 µm, D. 50 µm.
FIGURE 25 in Aplysina Nardo (Porifera, Verongida, Aplysinidae) from the Brazilian coast with description of eight new species
FIGURE 25: A–D. Aplysina solangeae sp.n. Holotype (MNRJ 4173). A–B. habit after preservation. C. Skeletal architecture. D. Spongin fibres. Scale bars = A–B. 1 cm, C. 500 µm, D. 50 µm.
FIGURE 9 in Aplysina Nardo (Porifera, Verongida, Aplysinidae) from the Brazilian coast with description of eight new species
FIGURE 9: A. Aplysina insularis (Duchassaing & Michelotti, 1864: 64). B. Aplysina alcicornis sp.n. in situ, Holotype – MNRJ 5473 (Parque Nacional Marinho dos Abrolhos, BA, Brazil). C. Aplysina cristagallus sp.n. in situ, Holotype— MNRJ 3528 (Prado, BA, Brazil). Scale bar = 1 cm.
FIGURE 11 in Aplysina Nardo (Porifera, Verongida, Aplysinidae) from the Brazilian coast with description of eight new species
FIGURE 11: Map showing the distribution of Aplysina along the Brazilian coastline. A. Aplysina insularis (Duchassaing & Michelotti, 1864) B. Aplysina lacunosa (Pallas, 1766). C. Aplysina pergamentacea Hechtel, 1983. D. Aplysina alcicornis sp.n.. Scale bar = 500 km.
FIGURE 7 in Aplysina Nardo (Porifera, Verongida, Aplysinidae) from the Brazilian coast with description of eight new species
FIGURE 7: A–C. Aplysina fulva (Pallas, 1766)—in situ. A. Neotype—MNRJ 7975 (Armação dos Búzios, RJ, Brazil). B–C. Salvador (BA, Brazil). Scale bar = 1 cm.
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