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13 results for “Continuous Rotation”
Continuous rotation electron diffraction data for Zeolite Mordenite
<p><strong>Raw continuous rotation electron diffraction data for mordenite:</strong><br> <br> - mordenite_cRED_1.zip<br> - mordenite_cRED_2.zip</p> <p>The zip file contains 3 directories<br> <br> - SMV: Diffraction data (stretch correction applied) in SMV format<br> - Tiff: Raw diffraction data in 16-bit unsigned integer TIFF format<br> - Defocused images in 16-bit unsigned integer TIFF format</p> <p>Experimental parameters are stored in the header files of the SMV images, and in the file cRED_log.txt<br> The SMV data can be processed using XDS.</p> <p><br> <strong>Raw serial electron diffraction data sets for mordenite:</strong></p> <p> - mordenite_SerialED.zip</p> <p>The zip file contains at least 3 directories:</p> <p> - calib: contains the calibration files for the experiment<br> - data: contains the raw diffraction data for all the identified crystals in hdf5 format<br> - images: contains the image data used to locate crystals in hdf5 format</p> <p>Experimental parameters (such as the crystal coordinates) are stored in the attributes on the data files. The Python code to process the data can be found in the problematic-0.1.0.zip folder or on http://github.com/stefsmeets/problematic<br> Prediction scores for all diffraction patterns are given in `learning.csv`<br> </p>
"Chirality and accurate structure models by exploiting dynamical effects in continuous-rotation 3D ED data". Raw data and JANA refinement files.
<p><strong>Chirality and accurate structure models by exploiting dynamical effects in continuous-rotation 3D ED data</strong><br> 3D ED data sets of 5 compounds and JANA refinement files of 12 compounds</p> <p><strong>Relevant tools</strong><strong>:</strong></p> <ul> <li>PETS2: data reduction and analysis of electron diffraction patterns <ul> <li>Download program and access step-by-step tutorials at <a href="http://pets.fzu.cz/">http://pets.fzu.cz/</a></li> <li>Palatinus, L. <em>et al.</em> Specifics of the data processing of precession electron diffraction tomography data and their implementation in the program PETS2.0. <em>Acta Cryst. B</em><strong>75</strong>, 512–522 (2019). <a href="https://doi.org/10.1107/S2052520619007534">DOI: 10.1107/S2052520619007534</a></li> </ul> </li> <li>JANA2006: crystal structure model refinement program <ul> <li>Download program from <a href="http://jana.fzu.cz/">http://jana.fzu.cz/</a> and access step-by-step tutorials at <a href="http://pets.fzu.cz/">http://pets.fzu.cz/</a></li> <li>Results here were obtained with JANA2006. We recommend using JANA2020.</li> <li>Petricek, V., Dusek, M. & Palatinus, L. Crystallographic Computing System JANA2006: General features. <em>Z. Kristallogr.</em> <strong>229</strong>, 345–352 (2014). <a href="https://doi.org/10.1515/zkri-2014-1737">DOI: 10.1515/zkri-2014-1737</a></li> </ul> </li> <li>DYNGO: Bloch wave program, calculates dynamical diffraction intensities and derivatives <ul> <li>Program automatically included in JANA2006/JANA2020</li> <li>Palatinus, L., Petříček, V. & Corrêa, C. A. Structure refinement using precession electron diffraction tomography and dynamical diffraction: theory and implementation. <em>Acta Cryst. A</em><strong>71</strong>, 235–244 (2015). <a href="https://doi.org/10.1107/S2053273315001266">DOI: 10.1107/S2053273315001266</a></li> </ul> </li> </ul> <p><strong>3D ED data sets:</strong></p> <p>STW_HPM-1 (RT) was measured on a JEOL JEM-2100-LaB6 and diffraction patterns were recorded with an ASI Timepix detector. Another sample of STW_HPM-1 was measured at a temperature of 100 K after cryotransfer with a Titan Krios (CETA-D detector). The other data sets were measured on an FEI Tecnai G2 20 (Olympus SIS Veleta, CCD). Each data set contains the raw diffraction patterns (*.tif) and the basic input files needed to reproduce the data reduction with PETS2 as used in the associated publication (*.pts2, *.celllist, *.cenloc). Step-by-step tutorials are provided for quartz and glycine (and selected steps for abiraterone acetate) at <a href="http://pets.fzu.cz/">http://pets.fzu.cz/</a>.</p> <ul> <li>α-quartz, stepwise continuous-rotation and precession-assisted (2 data sets from the same crystal)</li> <li>natrolite, stepwise continuous-rotation and precession-assisted (2 data sets from the same crystal)</li> <li>cobalt aluminophosphate (CAP), static ED patterns recorded in 0.1° steps (3 data sets from 2 crystals)</li> <li>abiraterone acetate, stepwise continous-rotation (5 data sets from 5 crystals)</li> <li>STW_HPM-1, continuous-rotation (1 data set, room temperature)</li> <li>STW_HPM-1, continuous-rotation (1 data set, <em>T</em> = 100 K, cryotransfer)</li> </ul> <p><strong>JANA refinement and CIF files:</strong></p> <p>CIF (Crystallographic Information Framework) files include two data items. The first is related to the dynamical and the second to the kinematical refinement. Relevant parameters and statistics specific for dynamical refinement are found in the field _refine_special_details.</p> <p>JANA files are provided for the dynamical and kinematical refinement at the stage after the final refinement cycle together with the original input files generated by PETS2. For quartz and natrolite, relevant files for the refinements against precession-assisted 3D ED data are included. For abiraterone acetate and limaspermidine, relevant files for the absolute structure determination are included.</p> <ul> <li>α-quartz</li> <li>albite</li> <li>mordenite</li> <li>natrolite</li> <li>STW_HPM-1</li> <li>cobalt aluminophosphate (CAP)</li> <li>CAU-36</li> <li>α-glycine</li> <li>carbamazepine</li> <li>(+)-limaspermidine</li> <li>abiraterone acetate</li> <li>MBBF4</li> </ul> <p>For the kinematical refinements based on more than one data set, the self-written tool "CompInt" (unpublished) was used. The tool can be found in the file "tool_scalehkl_compint.zip". Input (*.hkl, *.compint) and output files (*.scalehkl) are provided in the respective folder with the JANA files.</p> <p>Raw data sources of other data sets relevant for the associated publication are given in the SI of the associated publication.</p>
Continuous rotation electron diffraction data for zeolite SSZ-27
<p><strong>Raw data for SSZ-27 (as-synthesized)</strong></p> <p>The directories labeled <strong>S**</strong> contain the raw data for the SSZ-27 phase, those labeled <strong>C**</strong> for the SSZ-26 impurity.</p> <p>Each directory contains the following:</p> <ul> <li>cred_log.txt, data collection log file</li> <li>SMV, Directory with data in SMV format and XDS processing output</li> <li>tiff, Directory with raw data in TIFF format</li> <li>tiff_image, Directory with defocused images showing the position of the crystal</li> <li>pets.pts, input file for PETS</li> <li>beam_centers.txt, a table with the position of the primary beam</li> </ul> <p>Then there are three other directories:</p> <ul> <li>XSCALE, contains the scaling results from the 14 SSZ-27 crystals that were used for the cluster analysis</li> <li>SSZ-26_cluster_1, contains the clustering results and refinement data for SSZ-26</li> <li>SSZ-27_cluster_4, contains the clustering results and refinement data for SSZ-27</li> </ul> <p>The data were collected using the software <a href="https://github.com/stefsmeets/instamatic">instamatic</a> and processed using <a href="http://xds.mpimf-heidelberg.mpg.de/">XDS</a>/<a href="https://github.com/stefsmeets/edtools">edtools</a>.</p>
Serial Rotation Electron Diffraction (automated continuous RED) raw data sets
<p><strong>Serial Rotation Electron Diffraction (automated continuous RED) raw data sets </strong></p> <p>Containing:</p> <p>TIFF images for particle recognition</p> <p>SMV files for XDS processing</p> <p>XDS input files (automatically generated)</p>
Data for: How do harvesting methods applied in continuous-cover forestry and rotation forest management impact soil carbon storage and degradability in boreal Scots pine forests?
<p>Forest management affects soil carbon (C) storage through forest composition, microclimate and litter inputs. How two major forest management systems, continuous-cover forestry (CCF) and clear-cut-based rotation forest management (RFM), differ in their impact on soil C in boreal forests is still poorly understood, however. We compared their effects on soil organic carbon (SOC) storage and quality in boreal Scots pine <span>(<em>Pinus sylvestris</em></span> L.) dominated forests in eastern Finland. We tested the hypotheses that (1) colder microclimates and continuous litter inputs will lead to higher SOC stocks in CCF plots than in clear-cuts and (2) the more labile litter in clear-cuts with varying ground vegetation will enhance SOC decomposition rates. We sampled uncut mature forests, clear-cuts, retention-cuts and gap-cuts, in which we analysed SOC concentrations and calculated the stocks. We measured stand characteristics such as diameter-at-breast height, basal area, dominant tree height, and understorey species coverage of the various treatments and modelled the above- and belowground litter inputs based on these parameters. We used laboratory incubation and sequential fractionation of SOC to assess its degradability under standardized conditions. To estimate the decomposition rate in the various environments we incubated cellulose bags in situ. We assessed the impact of microclimate on SOC decomposition, using data from soil-temperature and soil-moisture field measurements. We quantified the microbial biomass C pool, using chloroform fumigation extraction to gain insight on the impact of forest management practice on soil microbes. The SOC concentrations and SOC stocks did not differ significantly between the treatments, despite the presence of a warmer microclimate and lower litter inputs in the clear-cut plots. However, we found differences in the quality of the SOC. Soils in clear-cut sites showed lower proportions of labile SOC compounds than did the other treatments. As hypothesized, the decomposition rates were elevated in clear-cuts, but were equally as high within the canopy gaps on gap-cut stands. Our work highlights that forest management affects the quality, degradability, long-term accumulation and storage of SOC. We conclude that the accumulation of labile compounds in uncut forests and retention-cuts, combined with the decreased decomposition rates, indicate a higher potential for future C accumulation in the soil than in clear-cuts.</p>
Data for: How do harvesting methods applied in continuous-cover forestry and rotation forest management impact soil carbon storage and degradability in boreal Scots pine forests?
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Ultrasound-guided Interscalene Brachial Plexus Block: Single Bolus Vs Continuous Catheter Placement in Arthroscopic Rotator Cuff Repair
ClinicalTrials.gov study NCT06855381. IPD Sharing: NO. Countries: 1. Publications: 1.
CORA-Q15: Continuous vs. Single-injection Interscalene Block on QoR-15 in Outpatient Rotator Cuff Surgery
ClinicalTrials.gov study NCT06754657. IPD Sharing: NO. Countries: 1. Publications: 14.
Incidence of Brachial Plexus Injury After Rotator Cuff Repair With Continuous Interscalene Block
ClinicalTrials.gov study NCT01334632. IPD Sharing: Not stated. Countries: 1. Publications: 0.
Single Shot vs Continuous Interscalene Block for Rotator Cuff Repair
ClinicalTrials.gov study NCT01122745. IPD Sharing: Not stated. Countries: 1. Publications: 0.
Rotator Cuff Failure With Continuity
ClinicalTrials.gov study NCT02716441. IPD Sharing: NO. Countries: 1. Publications: 0.
Prophylaxis of Ventilator Associated Pneumonia by Continuous Lateral Rotation Therapy
ClinicalTrials.gov study NCT00529776. IPD Sharing: Not stated. Countries: 1. Publications: 0.
Structure and variation in microbiome from continuous and rotational Pinellia ternata cropping soils
GEO Series GSE91083. uncultivated soil bacterium; Pinellia ternata. 54 samples. Type: Other.
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