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34 results for “Ion chromatography”

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zenodo44/100

IODP Expedition 391 Ion chromatography

Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.

opencc-by-4.0Oct 2023View details →
zenodo44/100

IODP Expedition 383 Ion chromatography

Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.

opencc-by-4.0Jul 2021View details →
zenodo44/100

IODP Expedition 378 Ion chromatography

Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.

opencc-by-4.0Feb 2022View details →
zenodo44/100

IODP Expedition 367 Ion chromatography

Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.

opencc-by-4.0Sep 2018View details →
zenodo44/100

IODP Expedition 379 Ion chromatography

Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.

opencc-by-4.0Feb 2021View details →
zenodo44/100

IODP Expedition 371 Ion chromatography

Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.

opencc-by-4.0Feb 2019View details →
zenodo44/100

IODP Expedition 397 Ion chromatography

Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.

opencc-by-4.0Jun 2024View details →
zenodo44/100

IODP Expedition 398 Ion chromatography

Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.

opencc-by-4.0Jul 2024View details →
zenodo44/100

IODP Expedition 355 Ion chromatography

Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.

opencc-by-4.0Aug 2016View details →
zenodo44/100

IODP Expedition 356 Ion chromatography

Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.

opencc-by-4.0Feb 2017View details →
zenodo44/100

IODP Expedition 353 Ion chromatography

Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.

opencc-by-4.0Jul 2016View details →
zenodo44/100

A Gas Chromatography – Ion Mobility Spectrometry dataset for colorectal cancer diagnostic of 56 urine samples corresponding to 29 subjects.

<p><strong>Contents of the dataset</strong></p> <p>The dataset includes the set of urine samples in .mea format, which can be<br> read using the GCIMS R package.</p> <p>It also contains analytical standards in the same format, used for quality<br> control of the equipment and as a retention time alignment reference.</p> <p>If you want to preview the data, you do not need to download the full Urines.zip<br> and AnalyticalStandards.zip files, but rather use the smaller UrinesDemo.zip and<br> AnalyticalStandardsDemo.zip, with a subset of just three samples of the whole<br> dataset.</p> <p>Besides the actual measurements, you will find the annotations.csv and<br> reference_peaks.csv files, with sample annotations and some reference peaks<br> identified in the samples.</p> <p>See further details below.</p> <p><br> <strong>Sample collection</strong></p> <p>Urine samples from 29 subjects were collected at Hospital de Reus. 15 subjects<br> were diagnosed with colorectal cancer, 14 subjects were controls. The study<br> protocol was approved by the Ethics Committee of Hospital de Reus (study<br> approval no. 074/2018).</p> <p>Samples were aliquoted and frozen at -80&ordm;C for storage.</p> <p><strong>Sample preparation</strong><br> &nbsp;</p> <p>Sample preparation improves urine preservation by blocking bacterial growth in<br> the urine, and favours volatile extraction. It also adds an internal standard<br> for verification of instrument variability.</p> <p><em>Stock solution preparation</em></p> <p>Dissolve 11.69 g of NaCl in about 35 mL deionized water and add 6.5 mg sodium<br> azide (NaN3). Once dissolved, add 5.50 mL 5M HCl and mark up to volume with<br> deionized water until the final volume is 50mL. The HCl 5M is used to obtain<br> an acid pH. The pH is controlled with a pH test paper. The final pH level must<br> be 2 or below. The NaCl favors the volatile extraction, and the NaN3 omits<br> the bacterial growth in the urine.</p> <p><em>Internal standard solution preparation</em><br> &nbsp;</p> <p>The 4-flurobenzaldehyde is located in retention time around 200 seconds and<br> can be used as an internal standard.</p> <p>Prepare a methanol stock solution using 100 ml of methanol grade for<br> preparative chromatography and 200 ml of distilled water.</p> <p>Mix 5 mL of 4-fluorobenzaldehyde with 100 mL of the methanol stock solution.</p> <p>Dilute the previous mixture in 400 mL of mili-Q water.</p> <p><br> <em>Sample preparation</em><br> &nbsp;</p> <p>Aliquotes were thawed before analysis. Once thawed, 300uL of the stock solution<br> were added to the urine sample, and 1.5 ml of the acidified urine sample were<br> transferred into a 20ml vial, ensuring only the supernatant of the sample<br> is transferred.</p> <p>Finally, 20 mL of the internal standard solution is added to the sample.</p> <p><strong>GC-IMS Analysis</strong></p> <p>Samples were analyzed with a GC-IMS FlavourSpec&reg; instrument from<br> G.A.S. Dortmund (Dortmund, Germany). Samples were incubated for 15 minutes<br> at 60&ordm;C, the flow rate of the drift gas was set at 200 ml/min, and the carrier<br> gas was set 11 ml/min. Both the drift and carrier gas were Nitrogen 5.0. The GC<br> and IMS temperature were set at 60&ordm;C and the measurement time lasted 33 minutes.</p> <p>Besides the urines, a set of measurements of a ketone mixture was also analyzed<br> at least once per day as an analytical standard control of the equipment. The mixture<br> included 6 ketones (2-butanone, 2-pentanone, 2-hexanone, 2-heptanone,<br> 2-ocatanone and 2-nonanone). This mixture is measured in the same conditions as<br> the urine samples.</p> <p>Samples are provided in the native instrument format (.mea format), that can be<br> read with the GCIMS R package or with the instrument software.</p> <p><strong>Sample annotations</strong></p> <p>The dataset includes a CSV file with sample annotations.</p> <p>The annotations include the following information:</p> <ul> <li>Diagnostic: Either ColorectalCancer or Control</li> <li>Sex: Either Male or Female</li> <li>Sample volume (in ml)</li> <li>Fasting: Whether the sample was collected with the patient in fasting conditions</li> <li>Age in years</li> <li>Weight_kg</li> <li>Height_cm</li> <li>BMI</li> <li>Smoker: TRUE/FALSE, whether the patient smoked</li> <li>Diseases: Whether the patient suffered from ArterialHypertension, CardiacFailure, Cholesterol, Dyslipidemia, Fibromyalgia or Tuberculosis</li> <li>AnalysisDateTime: Date and time of the GC-IMS analysis of the sample</li> </ul> <p><br> <strong>Reference peaks</strong></p> <p>Some peaks were manually annotated to ease the alignment of the samples and explore<br> alignment solutions. While manual peak labelling is not generally required, we<br> attach those reference peaks as well and their locations, in case they are of<br> interest.</p> <p>These reference peaks are found at reference_peaks.csv.</p> <p>&nbsp;</p>

opencc-by-4.0Feb 2023View details →
zenodo40/100

IODP Expedition 362 Ion chromatography

<p>Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.</p>

opencc-zeroMar 2020View details →
zenodo40/100

IODP Expedition 366 Ion chromatography

<p>Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.</p>

opencc-zeroMar 2020View details →
zenodo40/100

IODP Expedition 374 Ion chromatography

<p>Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.</p>

opencc-zeroAug 2019View details →
zenodo40/100

IODP Expedition 352 Ion chromatography

<p>Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.</p>

opencc-zeroSep 2015View details →
zenodo40/100

IODP Expedition 351 Ion chromatography

<p>Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.</p>

opencc-zeroAug 2015View details →
zenodo40/100

Raw data for evaluation of Floral Volatile-Patterns in the Genus Narcissus using Gas Chromatography coupled Ion Mobility Spectrometry

<p>We used a commercial gaschromatography coupled ion mobility spectrometer, equipped with an integrated in-line enrichment system for fast, sensitive and automated analysis of floral volatile patterns in the genus <em>Narcissus</em>. The raw data of individual measurements are stored together with corresponding telemetry data as data matrices. The determined retention times and ion mobilities (series and columns) can be used for the identification of substances.&nbsp; The measured values (intensities) are used for a (semi)-quantoitative determination of individual substances.Based on these raw data, heatmaps can be generated in this way, which allow a comparison and potentially identification of floral volatiles.&nbsp;</p> <p>This data set is part of a proof of concept study for the use of GC-IMS in the investigation of flower volatiles.</p>

opencc-by-4.0Dec 2022View details →
zenodo40/100

IODP Expedition 350 Ion chromatography

<p>Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.</p>

opencc-zeroMay 2015View details →
zenodo40/100

IODP Expedition 376 Ion chromatography

<p>Cation and anion concentration in interstitial water samples was measured by ion chromatography using a conductivity detector. Cation analytes include calcium, magnesium, potassium, and sodium. Anion analytes include chloride, sulfate, and bromide.</p>

opencc-zeroJul 2019View details →

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