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15 results for “Laser diffraction”

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zenodo40/100

[Data] Acoustic emission signature of martensitic transformation in Laser Powder Bed Fusion of Ti6Al4V-Fe, supported by operando X-ray diffraction

<p>The dataset for this study focuses on investigating Acoustic Emission (AE) monitoring in the Laser Powder Bed Fusion (LPBF) process, using premixed Ti6Al4V-(x wt%) Fe, where x = 0, 3, and 6. By employing a structure-borne AE sensor, we analyze AE data statistically, uncovering notable discrepancies within the 50-750 kHz frequency range. Leveraging Machine Learning (ML) methodologies, we accurately predict composition for particular processing conditions. These fluctuations in AE signals primarily arise from unique microstructural alterations linked to martensitic phase transformation, corroborated by operando synchrotron X-ray diffraction and post-mortem SEM and EBSD analysis. Moreover, cracks are evident at the periphery of the printed parts, stemming from local inadequate heat input during the blending of Ti6Al4V with added Fe powder. These cracks are discerned via AE signals subsequent to the cessation of the laser beam, correlating with the presence of brittle intermetallics at their junction. This study highlights for the first time the potential of AE monitoring in reliably detecting footprints of martensitic transformations during the LPBF process. Additionally, AE is shown to prove valuable for assessing crack formations, particularly in scenarios involving premixed powders and necessitating precise selection of processing parameters, notably at part edges.</p>

opencc-by-4.0Nov 2024View details →
zenodo40/100

Predicting Pulsed Laser Deposition SrTiO3 Homoepitaxy Growth Dynamics using High-Speed Reflection High-Energy Electron Diffraction - sample treated_213nm

<p>RHEED intensity image dataset of sample &quot;<strong>treated_213nm&quot;</strong> in work &quot;Predicting Pulsed Laser Deposition SrTiO<sub>3 </sub>Homoepitaxy Growth Dynamics using High-Speed Reflection High-Energy Electron Diffraction.&quot;</p>

opencc-by-4.0Apr 2023View details →
zenodo40/100

Datasets for Work "Predicting Pulsed-Laser Deposition SrTiO3 Homoepitaxy Growth Dynamics using High-Speed Reflection High-Energy Electron Diffraction"

<p>RHEED raw dataset and Gaussia fitting&nbsp;parameter dataset for&nbsp;samples &quot;treated_213nm&quot;, &quot;treated_81nm&quot; and &quot;untreated_162nm&quot;&nbsp;in&nbsp;the work &quot;Predicting Pulsed Laser Deposition SrTiO<sub>3 </sub>Homoepitaxy Growth Dynamics using High-Speed Reflection High-Energy Electron Diffraction.&quot;</p>

opencc-by-4.0May 2023View details →
dryad36/100

Evidence for phonon hardening in laser excited gold using x-ray diffraction at a hard x-ray free electron laser

<p>Studies of laser-heated materials on femtosecond timescales have shown that the interatomic potential can be perturbed at sufficiently high laser intensities. For gold, it has been postulated to undergo a strong stiffening leading to an increase of the phonon energies, known as phonon hardening. Despite efforts to investigate this behavior, only measurements at low absorbed energy density have been performed, for which the interpretation of the experimental data remains ambiguous. By using in situ single-shot x-ray diffraction at a hard x-ray free electron laser, the evolution of diffraction line intensities of laser-excited Au to a higher energy density provides evidence for phonon-hardening.</p>

opencc-zeroJan 2024View details →
zenodo36/100

ODP Site 1249, ODP Site 1252, and IODP Site U1325: X-ray fluoresence core scanning, laser diffraction grain size, CNS elemental/isotopic, environmental magnetism, and age model data

<p>We present data used as part of an integrative early diagenesis study (submitted September 2022 to Marine Geology) focused on identifying zones of magnetite dissolution and pyrite precipitation in which magnetic susceptibility records are altered in gas-hydrate bearing sediments on the Cascadia Margin using archived cores from the Ocean Drilling Program (ODP) and Integrated Ocean Drilling Program (IODP). We analyzed the upper 85 to 100 m below seafloor (mbsf) from ODP Sites 1249 and 1252, and IODP Site U1325. ODP 1249 is at the summit of Hydrate Ridge in an area of active methane seepage and massive gas hydrate accumulations and ODP 1252 is in a nearby slope basin with little occurrence of hydrate. IODP Site U1325 is on the northern Cascadia Margin in a slope basin, with turbidite-hosted gas hydrate. We also include XRF data from the upper sections of ODP Site 1251, IODP U1327, and U1328.</p> <p>We measured X-ray fluorescence using an Avaatech core scanner at the IODP Gulf Coast Repository at Texas A&amp;M University. We measured total carbon, total organic carbon (TOC), total nitrogen, and total sulfur using a Perkin Elmer 2400 Series CHNS/O Analyzer at the university of New Hampshire (ODP Site 1249 and 1252 only). A subset was analyzed for &delta;<sup>13</sup>C-TOC using a Costech ECS 4010 elemental analyzer interfaced with a Thermo Finnegan Delta Plus XP continuous flow isotope ratio mass spectrometer at Washington State University. Grain size was measured with a Malvern Mastersizer 2000 laser diffraction particle size analyzer and Hydro 2000G dispersal unit at the University of New Hampshire. Mass frequency-dependent magnetic susceptibility was measured using a Bartington MS2 Magnetic Susceptibility Meter and Bartington MS2B dual frequency sensor (Site U1325 only). Isothermal remanent magnetization and thermal demagnetization curves were measured using a HSM2 SQUID-based Spinner Magnetometer with an ASC Scientific IM-10-30 Impulse Magnetizer and ASC Scientific TD-48SC magnetically-shielded oven (Site U1325 only). Radiocarbon was measured on mixed planktic foraminifers at the Radiocarbon was measured at National Ocean Sciences Accelerator Mass Spectrometry (NOSAMS) facility at Woods Hole Oceanographic Institution (ODP Site 1252 and IODP Site U1325).. Radiocarbon ages were calibrated to calendar ages using CALIB 8.2 and the Marine20 calibration curve. For ODP Site 1252 we used a reservoir correction of 230 &plusmn; 50 years (Yaquina Bay, Oregon, USA) and for IODP Site U1325 we used a reservoir correction of 202 &plusmn; 50 years (Amphitrite Point, British Columbia, Canada).&nbsp; &delta;<sup>18</sup>O was measured on benthic foraminifer <em>Uvigerina peregrina</em> tests using a Finnegan MAT 252 isotope ratio mass spectrometer with Kiel III device at the Oregon State University Stable Isotope Laboratory (ODP 1252) and a Finnegan MAT 253 isotope ratio mass spectrometer with Kiel IV device at the University of Michigan Stable Isotope Laboratory (ODP Site 1249 and IODP Site U1325).</p>

opencc-by-4.0Sep 2022View details →
zenodo36/100

Predicting Pulsed Laser Deposition SrTiO3 Homoepitaxy Growth Dynamics using High-Speed Reflection High-Energy Electron Diffraction - sample untreated_162nm

<p>RHEED intensity image dataset of sample <strong>untreated_162nm</strong> in work &quot;Predicting Pulsed Laser Deposition SrTiO<sub>3 </sub>Homoepitaxy Growth Dynamics using High-Speed Reflection High-Energy Electron Diffraction.&quot;</p>

opencc-by-4.0Apr 2023View details →
zenodo36/100

Predicting Pulsed Laser Deposition SrTiO3 Homoepitaxy Growth Dynamics using High-Speed Reflection High-Energy Electron Diffraction - sample treated_81nm

<p>RHEED intensity image dataset of sample <strong>t0.08</strong>&nbsp;in work &quot;Predicting Pulsed Laser Deposition SrTiO<sub>3 </sub>Homoepitaxy Growth Dynamics using High-Speed Reflection High-Energy Electron Diffraction.&quot;</p>

opencc-by-4.0Apr 2023View details →
zenodo36/100

Predicting Pulsed-Laser Deposition SrTiO3 Homoepitaxy Growth Dynamics using High-Speed Reflection High-Energy Electron Diffraction - gaussian_fit_parameters - sample untreated_162nm

<p>RHEED raw dataset and Gaussia fitting&nbsp;parameter dataset for&nbsp;sample &quot;untreated_162nm&quot; in work &quot;Predicting Pulsed Laser Deposition SrTiO<sub>3 </sub>Homoepitaxy Growth Dynamics using High-Speed Reflection High-Energy Electron Diffraction.&quot;</p>

opencc-by-4.0May 2023View details →
zenodo36/100

Compressed Datasets for Work "Predicting Pulsed-Laser Deposition SrTiO3 Homoepitaxy Growth Dynamics using High-Speed Reflection High-Energy Electron Diffraction"

<p>Compressed version of RHEED image datasets and Gaussia fitting&nbsp;parameter datasets for&nbsp;samples &quot;treated_213nm&quot;, &quot;treated_81nm&quot; and &quot;untreated_162nm&quot;&nbsp;in&nbsp;the work &quot;Predicting Pulsed Laser Deposition SrTiO<sub>3 </sub>Homoepitaxy Growth Dynamics using High-Speed Reflection High-Energy Electron Diffraction.&quot;</p>

opencc-by-4.0May 2023View details →
dryad36/100

Evidence for phonon hardening in laser excited gold using x-ray diffraction at a hard x-ray free electron laser

Open the record for dataset details and reuse information.

publicJan 2024View details →
dryad32/100

Data from: Making soil particle size analysis by laser diffraction compatible with standard soil texture determination methods

The standard sieving, pipette and hydrometer methods for soil particle size analysis (PSA) have three main drawbacks: procedures are tedious, time-consuming, and the results are protocol-dependent. Laser diffraction PSA delivers rapid results using standardized procedures, but so far it has been difficult to reconcile results with those from standard sedimentation methods. The objective of this study was to develop a protocol that would permit direct usage of laser diffraction PSA and render results compatible with current methods. The protocol was developed using standard soil samples from different textural classes. Regression of the laser diffraction PSA against the hydrometer/pipette method yielded coefficients of determination of 0.92/0.9, 0.92/0.94 and 0.99/0.99, and root mean square errors of 0.04/0.05, 0.07/0.06 and 0.05/0.03 for clay, silt and sand, respectively. These statistics are comparable to those obtained by regressing results of the hydrometer against the sieve and pipette methods. A key factor in securing accurate and precise results was limiting the particle size range of the samples by wet sieving the sand fraction. This created representative samples and stable soil dispersed suspensions, allowing accurate estimations of particle size distribution for clay and silt fractions without empirical transformations. Results obtained with the proposed protocol matched those of standard sedimentation analyses for a wide range of soils, encouraging further adoption of laser diffraction for soil PSA.

opencc-zeroDec 2019View details →
zenodo32/100

Data to reproduce the results presented in de Lange et al. 2023. Water Resources Research, "The Impact Of Flocculation on In Situ and Ex Situ Particle Size Measurements by Laser Diffraction"

<p>This repository&nbsp;consists data to reproduce results as presented in:&nbsp;"The Impact Of Flocculation on In Situ and Ex Situ Particle Size Measurements by Laser Diffraction", Water Resources Research. Kindly refer to the readme.text file to navigate through&nbsp;the dataset.</p>

opencc-by-4.0Dec 2022View details →
dryad32/100

Data from: Making soil particle size analysis by laser diffraction compatible with standard soil texture determination methods

Open the record for dataset details and reuse information.

publicDec 2019View details →
dryad28/100

Data from: Making soil particle size analysis by laser diffraction compatible with standard soil texture determination methods

Open the record for dataset details and reuse information.

publicMay 2020View details →
ClinicalTrials.gov24/100

Enhanced Photoaging Reversal Efficacy and Safety of 755nm Alexandrite Picosecond Laser with Diffractive Lens Array (DLA) in Conjunction with Integrated Skin Care for Skin Quality Improvement

ClinicalTrials.gov study NCT06818630. IPD Sharing: NO. Countries: 1. Publications: 0.

closedIPD-NOFeb 2026View details →

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