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4 results for “Solid state processing”
NMR assignment of methyl groups in solid-state using 1H-detection and fast MAS - NMR raw and processed data
<p>This data set contains raw NMR data in Bruker format for experimental series on (1) 2,3-13C-labelled microcrystalline alanine, (2) U-13C,15N-labelled N-fomylated microcrystalline tripeptide Met-Leu-Phe, and (3,4) two differently labelled (ILV-C4 and ILV-C5) microcrystalline chicken-alpha-spectrin SH3 domain. Measurements were performed at 14.4 T and 55.5 kHz MAS (alanine), 18.8 T and 55.5 and 98 kHz MAS (fMLF), 23.5 T and 55.5 kHz (SH3 C5), 18.8T and 55.5 and 94.5 kHz MAS (SH3 C5) and 18.8T and 55.5 and 94.5 kHz MAS (SH3 C4). The data set also contains Fourier processed data (spectra) in UCSF format, Sparky project, save and peak list files. Pulse programs for Bruker spectrometers are provided. The data set is complemented with SIMPSON scripts for simulation of spin dynamics under aformentioned conditions.</p>
Photoluminescence processes in τ-phase Dy3+/Tb3+-codoped Ba1.3Ca0.7SiO4 phosphors for solid-state lighting
<p>The τ-phase-Ba<sub>1.3</sub>Ca<sub>0.7</sub>SiO<sub>4</sub> phosphors co-doped with 3 mol% Dy<sup>3+</sup> and ~1-5 mol% Tb<sup>3+</sup> trivalent rare-earth ions were prepared by the gel-combustion method. The structure-property relation of the samples was examined by X-ray diffraction, scanning electron microscopy, and spectrophotometer. Here, the effect of Tb<sup>3+</sup>'s concentration on the spectroscopic properties of Dy<sup>3+</sup>/Tb<sup>3+</sup> co-doped Ba<sub>1.3</sub>Ca<sub>0.7</sub>SiO<sub>4</sub> phosphors was explored by using the photoluminescence excitation, emission, and decay curves. Importantly, the photonic energy transfer from (Dy<sup>3+</sup>: <sup>4</sup>F9/2 + Tb<sup>3+</sup>: <sup>7</sup>F<sub>6</sub>) to (Dy<sup>3+</sup>: <sup>6</sup>H<sub>15/2</sub> + Tb<sup>3+</sup>:<sup>5</sup>D<sub>4</sub>) was observed, in which the Dy<sup>3+</sup> ions acts as a light-emitting donor whereas the Tb<sup>3+</sup> ions as a light-absorbing acceptor, resulting in an enhanced emission from the co-doped Ba<sub>1.3</sub>Ca<sub>0.7</sub>SiO<sub>4</sub>: Dy<sup>3+</sup>/Tb<sup>3+</sup> phosphors. Finally, the chromaticity coordinates were determined from the measured emission spectra, locating at the green and white light regions. This observation indicates that the characteristic emission color could be tuned from white to green by varying Tb<sup>3+</sup> concentrations under ultraviolet light.</p>
Photoluminescence processes in τ-phase Dy3+/Tb3+-codoped Ba1.3Ca0.7SiO4 phosphors for solid-state lighting
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Evaluation of solid state of rice flours produced by different milling processes using ATR-FTIR spectroscopy
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