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3 results for “reflection anisotropy spectroscopy”
Dataset for "Operando Investigation of Al Plating Regimes on HOPG in [EMImCl]:AlCl3 by Electrochemical Reflection Anisotropy Spectroscopy"
<p>This is the experimental raw data set associated with the following publication: M. Löw, and MM May, Operando Investigation of Al Plating Regimes on HOPG in [EMImCl]:AlCl3 by Electrochemical Reflection Anisotropy Spectroscopy, Batteries & Supercaps (2024). DOI:<span>10.1002/batt.202400610</span></p> <p>The data set is organized according to the publication's figures. </p>
Data set for "The interfacial structure of InP(100) in contact with HCl and H2SO4 studied by reflection anisotropy spectroscopy"
<p>This is the experimental raw data set associated with the following publication: M. Löw, M. Guidat, J. Kim, and MM May, <em>The interfacial structure of InP(100) in contact with HCl and H<sub>2</sub>SO<sub>4</sub> studied by reflection anisotropy spectroscopy</em>, RSC Advances 12 (2022), 32756-32764. <a href="https://doi.org/10.1039/D2RA05159A">DOI:10.1039/D2RA05159A</a></p> <p>The data set is organised along the figures of the publication. '.ers', '.erc', and '.ert' are spectra, colour plots, and transients, respectively, in the native format of Laytec's EpiRAS. '.par' files are in the data format from the Princeton Applied Research VersaSTAT 3F potentiostat. Spectra files containing the name 'Si100' are from Si(100) wafers with native oxide, used for zero-line correction as described in the paper.</p>
Dataset for publication "In Situ Monitoring of the Al(110)-[EMImCl]:AlCl3 Interface by Reflection Anisotropy Spectroscopy"
<p>Dataset are obtained from Reflection anisotropy spectroscopy, CV, SEM/EDX, and computaitonal RAS</p><p>The data are sorted according to the Figures of the paper.</p><p>Abstract of the paper:</p><p>Recently, Al-batteries (AlBs) have become promising candidates for post-lithium batteries, with [EMImCl]:AlCl3 (1:1.5) as the most commonly used electrolyte. However, progress in the development of AlBs is currently hindered by the lack of understanding of its solid-electrolyte interface. Monitoring the structure of this interface under operational conditions by complementary spectroscopy could help to identify and overcome bottlenecks of the system. Reflection anisotropy spectroscopy (RAS), an optical in situ technique, provides access to physical and chemical properties of electrochemical interfaces on an atomistic level. Herein, we report the first example of RAS as an in situ characterization technique for non-aqueous battery systems, investigating an Al(110)-based model system. During chemical pre-treatment in [EMImCl]:AlCl3 , the Al(110) surface passivation film is modified. The oxide film is partially etched while an inhomogeneous passivation layer forms, increasing the surface roughness. Upon electrochemical cycling, applied potential-dependent oscillations of the anisotropy are observed and demonstrate the applicability of RAS to monitor phenomena such as plating/stripping and surface passivation in real-time.</p>
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