Glove-Box ICP-OES Spectrometer for Controlled-Atmosphere Work
ICP-OES integrated into a glove box for air-sensitive and radiologically controlled samples.
Louise Corscadden, PhD
Director of Science · ConductScience
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Key Specifications
Full details →- RF power range
- 500-1600W continuous and adjustable
- RF power stability
- ≤0.1%
- RF frequency stability
- ≤0.01%
- Peristaltic pump
- 4-channel, 12-rotor
- Argon-flow control accuracy
- 0.01L/min
- Optical-chamber temperature
- 36°C
An optical emission spectrometer enclosed in a controlled-atmosphere glove box, keeping air-sensitive and contained material inside the barrier through the whole measurement rather than only up to the autosampler.
Key features
- Integrates optical emission spectrometry with a sealed glove-box work area.
- Vertical-torch plasma observation and array detection support multi-element analysis.
- A stainless-steel enclosure and transfer chamber maintain the controlled sample boundary.
Choosing the right configuration
Match the sample matrix and target elements to the required detection limits, sample-introduction hardware, gas supply, exhaust, cooling, and data-system configuration. ConductScience confirms these items against the proposed method before the system is quoted.
Features & Benefits
RF power range
- 500-1600W continuous and adjustable
RF power stability
- ≤0.1%
RF frequency stability
- ≤0.01%
Peristaltic pump
- 4-channel, 12-rotor
Argon-flow control accuracy
- 0.01L/min
Optical-chamber temperature
- 36°C
Optical-chamber fluctuation
- <0.2℃
Optical slit sizes
- 50 microns and 100 microns
Detector cooling
- -45°C
Glove-box sealing level
- level 2
Plasma observation
- vertical observation
Stray light
- ≤2.0 mg/L
Optical resolution
- ≤7 pm @200 nm
Precision
- RSD ≤1.0%
Two-hour stability
- RSD ≤1%@2h
Detection limits
- Zn 1 ppb; Ni 1 ppb; Mn 0.5 ppb; Cr 1 ppb; Cu 2 ppb; Ba 1 ppb
Glove-box material
- SUS304 stainless steel, 3mm
View-window thickness
- 8mm tempered glass
Glove openings
- two stainless steel openings
Transition-chamber material
- SUS304 stainless steel, 3mm
Reserved interfaces
- four KF40 standard interfaces
ICP-OES glove box callout
- The ICP-OES is combined with the glove box, providing the radial view with the vertical torch; the special large-area array high-sensitivity ECCD sensor is equipped to practically fulfill the full-spectrum once-for-all acquisition and complete the analysis of 72 elements quickly.
What does this instrument measure, and who is it for?
It measures major and trace elements in samples that must remain inside a sealed or protective enclosure. It is built for nuclear, battery and air-sensitive materials laboratories. It is a benchtop instrument intended for continuous laboratory duty, with a plumbed gas supply and extraction over the source.
What measurement principle does it use?
The sample-introduction path and torch interface remain inside a sealed glove-box boundary. An argon plasma excites the sample, and the optical system resolves element-characteristic emission while the sample-contact components remain contained.
Which specifications are confirmed?
The specification table lists twenty-two confirmed ordering parameters for this instrument. Use them to compare the operating range, utilities, and analytical performance required by the method. They include RF power range at 500-1600W continuous and adjustable, RF power stability at ≤0.1% and RF frequency stability at ≤0.01%.
What should be confirmed before ordering?
Confirm argon supply and purity, exhaust extraction over the torch or spark stand, single-phase power and breaker rating, bench load rating, and cooling water where the design requires it. These are configured and quoted per installation, so raise anything unusual about the site during quote review rather than after delivery.
What else is needed to run it?
A microwave digestion system, unless your samples already arrive in solution. Elemental analysis is only as good as the dissolution that preceded it, and an incomplete digest reports a low result with no indication that anything went wrong.
How is it supplied?
This instrument is configured and quoted per installation rather than sold at a list price. Request a quote and we will confirm the configuration, the site requirements and the lead time before anything is ordered.
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